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2B0-023 | ES Advanced Dragon IDS

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2B0-023 - ES Advanced Dragon IDS - braindump

Vendor Enterasys
Exam Number 2B0-023
Exam Name ES Advanced Dragon IDS
Questions 50 Q & A
Recent Update October 9, 2018
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2B0-023 exam Dumps Source : ES Advanced Dragon IDS

Test Code : 2B0-023
Test Name : ES Advanced Dragon IDS
Vendor Name : Enterasys
Q&A : 50 Real Questions

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Enterasys Enterasys ES Advanced Dragon

Enterasys Networks' Dragon Intrusion protection system Named IDS made from the year by using tips security magazine | killexams.com Real Questions and Pass4sure dumps

ANDOVER, Mass.--(business WIRE)--Dec. 15, 2004--   Award coincides with instant availability of Dragon 7.0; principal liberate marks subsequent technology in IDS/IPS efficiency, manageability and attain  

Enterasys Networks(R) (NYSE: ETS), the at ease Networks enterprise(TM), today introduced that its Dragon(R) Intrusion defense system has won the Gold award for IDS made from the yr from assistance safety journal. The award is in line with the votes of more than four hundred information protection professionals.

information safety noted Dragon "epitomizes the transition of IDSes from 'reactive detection' to 'proactive correlation.' in place of firing off hundreds of indicators in line with single-node scanning, Dragon makes use of distinct virtual sensors to correlate adventure records from throughout the network and compare it to gathered information on the networks' vulnerability posture. The process, managed through Enterasys' Dynamic Intrusion Response (DIR) equipment, results in more correct and well timed intrusion management, in addition to fewer false positives."

the respect comes as the company pronounces the instant availability of the newest and most comprehensive replace in the product's heritage--Dragon 7.0--which establishes a brand new benchmark in IDS/IPS performance.

The journal goes on to assert that "many companies are reluctant to put into effect full-scale inline IPS for worry of blocking off professional site visitors. Some clients imply that Dragon's passive scanning mixed with DIR assault correlation, is a extra good method."

Dragon got the Gold award in accordance with the opinions of satisfied purchasers, together with the CISO of a govt agency who said, "Enterasys is an imaginative enterprise that understands safety, and the way to protect you. it is inclined to work with diverse organizational wants."

information security additionally observed, "Enterasys has converted Dragon from a stand-on my own IDS to the cornerstone of its community safety structure."

"it's a fine honor for Dragon and Enterasys to receive such significant business attention. it's notably pleasant that the winner will depend on network and safety gurus who take note what it takes to be certain enterprise continuity with a sturdy and totally cozy infrastructure," noted Cynthia Gallant, senior vice chairman, at ease Networks community for Enterasys. "Now, with Dragon 7.0, we are delivering much more effective IDS performance to assist firms give protection to their vital network property from threats and unauthorized entry."

The 2004 items of the year awards have been according to the outcomes of interviews with more than 400 safety managers from 273 agencies. The InfoPro, an impartial analyst firm, compiled the results. each and every vendor is judged on its company or reputation, quality of product, start of product as promised, great of technical assist, technical innovation, strategic vision, aggressive positioning, nice of the earnings team, interoperability and ease of doing company.

Dragon 7.0

With the immediate availability of Dragon edition 7.0, Enterasys as soon as again raises the bar for business network security by way of providing the business's most robust intrusion-protection capabilities. Its interesting threat-detection know-how discovers threats, community misuse, gadget exploits and a wide selection of other malicious actions that can disrupt enterprise continuity, costing firms time and cash and adversely affecting the capability to satisfy valued clientele' wants. latest consumers and people wishing to consider the product can down load the application at https://dragon.enterasys.com/.

among the many key enhancements in Dragon 7.0 are:

-- next-technology management--person-friendly interface with role-based entry designed for scalability to satisfy the needs of organisations and managed protection carrier providers. a new GUI built on a Java framework in a shopper-server architecture promises ease of use, simplified configuration and centralized management of all Dragon facets.

-- excessive-performance architecture--a new multi-threaded structure makes it possible for proper Gigabit-per-second efficiency network sensors. The multifaceted engine provides possibility detection the usage of advanced signature-based pattern analysis, anomaly detection and protocol decoding.

-- virtual Sensors--allows for a single sensor to function as dissimilar entertaining sensors with wonderful guidelines and configurations, thereby limiting a client's deserve to buy assorted network IDS home equipment.

-- net Server Intrusion Prevention--Enterasys' first intrusion-prevention know-how is designed to offer protection to commercial enterprise internet servers. The Dragon net Intrusion Prevention know-how is essentially the most comprehensive and versatile internet server insurance plan product in the marketplace. It displays more points inside http communications than every other product and supports numerous response capabilities once an assault is found.

The Enterasys relaxed Networks advantage

Enterasys' business-leading cozy Networks technology and solutions supply the optimum level of infrastructure protection purchasable nowadays. cozy Networks gives you the most granular degree of security, presenting visibility and manage down to the community equipment, particular person consumer and application degree. This allows for firms to immediately and simply observe, investigate, find and protect against assaults. This unmatched protection comes from the integrated policy-based management software architecture that works with the embedded security capabilities Enterasys designs into its entire product line. This pleasing strategy offers big operational and business merits, unmatched via seller choices that add hardware or software to varied community access elements in an attempt to increase protection. really, at ease Networks expertise may also make networks with rivals' machine extra relaxed.

About Enterasys Networks

Enterasys Networks is the comfortable Networks enterprise, offering commercial enterprise consumers with imaginitive network infrastructure items, functions and solutions that convey the protection, productivity and flexibility merits required by international 2000 businesses. For extra suggestions on Enterasys at ease Networks and the enterprise's items, including multilayer switches, core routers, WAN routers, instant LANs, community administration, and intrusion defense programs, consult with www.enterasys.com.

This information liberate contains ahead-searching statements concerning future pursuits, activities and fiscal performance, comparable to administration's expectations concerning future salary and money move; strategic relationships and market opportunities; product development; and different business innovations and objectives. These statements may be identified with such phrases as "we predict," "we trust," "we count on," or equivalent signals of future expectations. These statements are neither promises nor guarantees, and precise future financial performance, routine and actions may also fluctuate materially. Readers are advised now not to place undue reliance on these statements, which communicate most effective as of the date hereof. We expressly disclaim any duty to update such statements publicly to replicate adjustments within the expectations, assumptions, hobbies or situations on which such statements can be based or that might also have an effect on the probability that actual effects will differ materially.

Some hazards and uncertainties that can cause exact outcomes to vary materially from these forward-looking statements consist of, but are not restrained to: worldwide and regional economic uncertainty and recent political and social turmoil may additionally continue to negatively affect our enterprise and earnings; we now have a heritage of losses in contemporary years and can not function profitably in the future; our quarterly operating effects may fluctuate, which might cause us to fail to satisfy quarterly working goals and effect in a decline in our stock cost; we earn a considerable portion of our earnings for each and every quarter in the ultimate month of each and every quarter, which reduces our means to precisely forecast our quarterly consequences and increases the chance that we might be unable to achieve up to now forecasted outcomes; we continue to introduce new products, and if our shoppers prolong product purchases or opt for alternative solutions, or if income of new products are not satisfactory to offset declines in revenue of older products, our income might decline, we can also incur extra and out of date inventory charges, and our financial circumstance may well be harmed; we may well be unable to upgrade our indirect distribution channels or otherwise boost our promoting capabilities, which may also prevent our potential to develop our customer base and enhance our revenue; we have experienced colossal alterations in senior administration and our present administration team has been collectively for under a confined time, which could limit our potential to obtain our objectives and comfortably function our enterprise; there is extreme competitors out there for enterprise network equipment, which might evade us from increasing our income and reaching profitability; a portion of the agencies we sell to count in entire or partially on public funding and infrequently face large budgetary drive, and if these consumers should lengthen, in the reduction of or forego deciding to buy from us, our revenues may be harmed; we depend on a restricted number of contract producers for substantially all of our manufacturing requirements, and the loss of any of our primary contract manufacturers would impair our capacity to fulfill the demands of our consumers; and people additional dangers and uncertainties discussed in our most contemporary filings with the Securities and trade commission, including our annual record on form 10-okay for the fiscal 12 months ended January three, 2004.


Milton Hershey school Deploys Enterasys comfy community to make sure legit network access for college students, faculty and body of workers throughout 200-building Campus | killexams.com Real Questions and Pass4sure dumps

Enterasys solution Ensures the optimum stages of security, efficiency, Visibility and control for rapidly transforming into network

ANDOVER, Mass., Feb. 26 // -- Enterasys Networks Inc., the at ease Networks company(TM), introduced today that Milton Hershey faculty has deployed an Enterasys secure community to make certain at ease, legit, excessive- performance community access to greater than three,000 college students and personnel. The infrastructure gives you connectivity and converged communications to more than 200 structures throughout its 3,000-plus-acre campus in Hershey, Pa.

founded in 1909 with the aid of chocolate industrialist Milton Hershey and his spouse, Catherine, the school opens new doorways for toddlers whose families couldn't otherwise find the money for a first class education. Milton Hershey faculty serves infants in fiscal and social want from all the way through the USA by way of proposing them schooling, housing, food, clinical and psychological fitness care, exercise opportunities, and apparel with out a financial responsibility to the family unit.

"we're in the middle of transforming into our community by way of 30 percent because of a tremendous expansion challenge involving new buildings and renovations to current facilities, so imposing a sturdy, scalable, and flexible network infrastructure to help our rapidly evolving needs become important," said Mike Bernardo, supervisor of networks and telecommunications for Milton Hershey faculty. "After an in-depth RFP preparation, thorough scorecard assessment, and certain demonstration, handiest Enterasys and its associate Comm options gave us the self assurance they might meet our necessities from day one. They in fact listened and worked closely with us to propose a confirmed answer that provided the crucial open-architecture interoperability, facets and functionality, with the flexibility to healthy the parameters of our capital and operating budgets. They delivered every thing they promised."

Milton Hershey college's Enterasys infrastructure comprises Matrix(TM) X excessive-availability relaxed routers on the core, redundantly connected by the use of four 10-Gbps hyperlink aggregation corporations (LAG) to Matrix N-series stream switches, which then distribute community capabilities to SecureStack C2 switches at the side by way of distinctive 1-Gbps LAGs. The college depends on Enterasys NetSight(R) for visibility and manage of its sprawling infrastructure, and Enterasys Dragon(R) to offer protection to the confidentiality, integrity and availability of information while decreasing the dangers associated with security threats and vulnerabilities.

"With its move-based mostly granularity the Matrix N-series change gives us in- depth discovery and prioritization of users and applications," pointed out Matt Hess, community engineer at Milton Hershey faculty. "It practically tells you greater than you could possibly ever deserve to learn about what's occurring on the community. or not it's effortlessly amazing!

"When there's an issue, the integrated hardware and utility answer from Enterasys allows for us to pinpoint the source right now and instantly verify the vicinity and impact. this saves us a massive amount of time and eliminates disruptions to network operations," referred to Hess.

The Enterasys cozy community supports the entire school's important facts- networking techniques, from safety (access, surveillance and emergency paging) to building administration programs (electric powered, gas, lighting, fireplace detection and HVAC) to clinical and dental methods. These services all function over the same infrastructure because the faculty's regular community functions, together with all enterprise and academic programs, wireless entry points and connections to more than 500 community printers and copiers.

"assist is an additional critical element of our relationship with Enterasys considering that nothing works with out the network," said Hess. "whether it is on the mobile, internet, email or on-website, responses are very quickly and accurate and we admire the very own contact from our local Enterasys answer engineer, their client-centric perspective, and our potential to get to the appropriate grownup appropriate away."

With its geographically dispersed campus and only two community engineers, Milton Hershey school values the manageability and safety embedded in the Enterasys solution. "We wanted an answer with a single management interface to enable quick troubleshooting, fault isolation, and automatic fix and that's precisely what we get with NetSight," said Hess. "different providers' solutions required administration utility that was so cumbersome and complicated we would have essential an additional full-time employee simply to manipulate the management system. NetSight is meeting our ambitions to be enormously intuitive, easy to make use of, and present the entire critical assistance about our community in a single location. We can also replace guidelines instantly to make sure security and QoS right down to the user, application and machine stage to assist assure community uptime."

sooner or later, Milton Hershey faculty will enhance its safety posture by means of further leveraging Enterasys' Dragon protection Suite. "We predict to fully put into effect Dragon later this 12 months, after we now have our coverage absolutely described out to the community edge. "The dashboard is so effective that even the effects now we have seen up to now with restrained implementation had been very fabulous," pointed out Hess. "Dragon's new graphical user interface simplifies operations and provides 'drill-down' capabilities that could be especially useful in our ambiance." in addition, the faculty expects to installation Enterasys' school room control answer to enable lecturers to make use of the most superior applied sciences while making certain complete handle over how college students use expertise and entry the cyber web in the classroom.

Bernardo says any okay-12 school can improvement from the unique at ease Networks capabilities provided by Enterasys. "Milton Hershey college has discovered a true recommend in Enterasys Networks. They took the time to keep in mind our environment, tackle our concerns, develop a cost-beneficial structure that met or exceeded all of our certain needs, and-most significantly-they committed to being our accomplice for the future."

About Enterasys Networks

Enterasys Networks--the at ease Networks business--is owned through a personal investor community led by way of The Gores group, LLC and Tennenbaum Capital partners, LLC. Enterasys' exciting comfortable Networks options cozy any community from any vendor and make sure the integrity and performance of IT capabilities and the business users that rely on them. lots of main organizations, government groups and academic institutions in more than 70 nations count on secure Networks options to hold enterprise continuity and offer protection to a must-have information. The company's subculture is headquartered on the precept "there's nothing more vital than our consumers." supplying on that commitment, relaxed Networks provides granular, coverage-based mostly command and control of particular person user, software, device, port and movement efficiency, and security. Enterasys' architectural method to network safety offers an extended technology lifecycle and critical operational and enterprise benefits, while reducing total can charge of possession. information about Enterasys' award-profitable policy- enabled switches, routers, instant items, safety software, and capabilities is attainable at www.enterasys.com.

concerning the Gores community

headquartered in 1987, The Gores group is a private fairness firm concentrated on acquiring controlling pursuits in mature and growing to be businesses which could benefit from the firm's working adventure and versatile capital base. The firm combines the operational knowledge and targeted due diligence capabilities of a strategic purchaser with the professional M&A group of a standard financial buyer. The Gores group has develop into a leading investor, basically within the know-how and telecommunications sectors, having proven over time a legit track record of growing big price in its portfolio organizations alongside management. Headquartered in la, California, The Gores group continues workplaces in Boulder, Colorado and London. For greater assistance, please discuss with www.gores.com.

About Tennenbaum Capital companions, LLC

Tennenbaum Capital companions is a Santa Monica, California-based mostly private investment enterprise managing over $3.eight billion in assets through private funds. The enterprise's investment approach is grounded in a protracted-term, price method, and it assists--both financially and operationally--transitional middle-market groups in such industries as know-how, healthcare, energy, aerospace, business capabilities, retail and general manufacturing. Tennenbaum's core strengths include its in-depth knowledge of equity and debt-financing cars in the public and private markets, as well as a radical figuring out of particular situations. For more information, please seek advice from www.tennenbaumcapital.com.

source: Enterasys Networks Inc.

CONTACT: Kevin Flanagan of Enterasys Networks, +1-978-684-1473, kevin.flanagan@enterasys.com

web web site: www.enterasys.com/http://www.tennenbaumcapital.com/http://www.gores.com/

connected Thomas business replace Thomas For Industry

Inseparable: Presence and Unified Communications | killexams.com Real Questions and Pass4sure dumps

October 14, 2008

with the aid of Richard Grigonis, govt Editor, IP Communications neighborhood

Unified Communications (information - Alert) devoid of presence is barely unified messaging with mobility. Presence can verify if an individual, at any moment, will also be contacted and how. in contact facilities, presence makes first name decision a reality, enabling a company knowledgeable to be discovered automatically who can assist close a sales name or get to the bottom of a client service inquiry. Presence saves time and raises productiveness by way of enabling clients to communicate more efficaciously throughout the complete company. in the most superior methods, presence tells you the place individuals are, what meeting they’re attending, and after they’ll be lower back at their desks. You can even be notified after they return to their desk or get off the mobilephone, making cellphone tag (information - Alert) and “voicemail detention center” a far off reminiscence. folks that pooh-pooh unified communications say that, in many situations, UC complicates things extra frequently than not, and doesn’t reside as much as its hype. Such naysayers may still take a look at Zeacom, which has worked with contact centers and enterprises for years, proposing budget friendly UC solutions that make high-conclusion features, corresponding to wealthy presence, mobility and Microsoft Outlook integration, accessible to small and medium-sized agencies, not have to massive ones.

prosperous presence is an quintessential part to Zeacom Communications middle 5.0; it gives you an entire view of your firm by featuring precise-time suggestions on the whereabouts and availability of personnel in spite of their vicinity. as an example, “Presence Pages” permit clients to view the status of all other users in the firm. These Presence Pages allow users to access world, personal and Microsoft Outlook Contacts buttons for one-touch and speed-dialing. users permit presence so that when they are within the workplace, their availability is recognized and displayed (“At my Desk”, “faraway from my Desk”) for all computing device and Console users throughout the network. A person is considered to be available in the event that they use their mouse, keyboard or telephone. After 10 minutes (or a configurable length) of state of being inactive, the user is considered to be away. in addition, laptop and console clients can request return notification for any presence user. This activates a screen pop to notify the user when the person they want to talk to turns into attainable.

If a consumer’s present Profile is ‘forwarded’ (i.e., the user’s cell is diverted to voice messaging) and their presence is detected, the computing device module pops a reminder to the user so we can update their Profile (e.g. alternate it to “within the workplace” which will acquire calls at their desk).  Presence clients can additionally decide to screen the discipline of their energetic Microsoft Outlook appointment for different users to view. this is peculiarly useful for keeping operators and receptionists recommended of team of workers whereabouts and availability.

probably the most first groups to make essential R&D efforts in both UC and presence changed into Avaya. Avaya lately unveiled new distributed UC solutions that aid each faraway workers and branch offices. Avaya says their new video-in a position Unified Communications for Teleworkers answer expenses below 15 cents per day per employee (when expenses are unfold over a three-year length).

Avaya will even be introducing almost immediately the Avaya one-X Communicator and Avaya intelligent Presence Server. Avaya one-X Communicator combines telephony capabilities, desktop video, visible voicemail, presence, e-mail, IM, convention bridge integration, directories, and phone history into one desktop customer software equipment that helps each SIP (Session Initiation Protocol) and H.323.

As for the Avaya clever Presence Server, it may mixture presence information from now not only Avaya programs however Microsoft’s and IBM’s too (it integrates with Microsoft workplace Communicator and change, and IBM Lotus Sametime). It supports SIP/SMPLE and XMPP.

given that presence is the adhesive of unified communications, it makes experience to talk to a UC issuer corresponding to Dialcom, which offer its Spontania, a true-time, business-grade, premise-based collaboration platform that seamlessly extends IM, voice, video and statistics in precise-time to any person, over any device or community, in spite of geographic area.

Dialcom’s President, Bob Johnson, says, “Spontania helps the execution by using any consumer of any number of verbal exchange modalities so she or he can collaborate with one or many individuals directly from the office, above all the computing device or an end-equipment comparable to a smartphone or a PDA. Spontania can take care of VoIP, so americans can speak with every other; it practically operates as a mobilephone bridge, if you will, directly off the pc. It helps video so you can share video. which you can share and switch data. that you would be able to act on a typical file, do a whiteboard, and so on. here is all tied into a presence engine that has its personal chat capacity too.”

“In a way,” Johnson continues, “the character of the utility resembles a middleware-enabler of a number of skill of verbal exchange that may additionally exist in a company and may be amplified via this, and if they don’t exist it in fact provides a few of these to the company. We don’t have ‘switchboard’ but we do work with switches, if you will, and we are able to pipe collaboration via general switches. We’ve had a couple of business method integrations where we installed this means and we were able to tie it right into a precise business application serving a contact center or some other ERP capacity, and by way of our tool, people can communicate tons easier than earlier than, as well as extra rapidly and more largely.”

“rapid messaging I consider has been slow to be adopted in enterprise, however is gaining floor because of the demographics that are transferring to young people, who've grown up with issues such as cellphones of their ears, in addition to social networks and chats” says Johnson. “those americans when within the workplace need to be aware of what this expertise can do for them, and the way they can socialize and work with other people.”

“What’s key's, if you happen to tie all of this into a business manner, you have to ask your self the way to get real contextual presence in accordance with field matter or a selected process inside a business method wherein you may well be engaged,” says Johnson. “who are the subject depend specialists, etc, and the way do you go from a normal presence engine to whatever thing that could be very particular focus, and the way to you convey that in so that i can have a very useful method of communicating with no need to seem to be people up somewhere and work out the way to communicate with them. and i believe context presence will be the one of the most wonderful issues in the future that starts to tie all of this together in a very dependent means, however I also suppose it’s a long way away. There are too many ‘transportable materials’ at the moment for many individuals to cope with. but when it definitely comes into being, it might be super, but we don’t have a solution for an choicest presence gadget yet.”

“yet another key aspect is the entire business of unified communications and collaboration,” says Johnson. “there are many the right way to strategy and outline these ideas, but there are so many ‘moving constituents’ to UC that I feel most groups are overwhelmed on the concept of it and don’t comprehend how to delivery adopting it let alone comprehend what they can benefit from it. there are such a lot of gamers in UC and collaboration that come at it from diverse angles, and yet all of them make the same claims, including us, really. however what we’ve been in a position to do as a corporation is to say, ‘seem to be, we don’t have each piece that you just want, but we now have a way to seek advice from most of those pieces and we now have a method to unify some of these inside your organization so that you can in reality use them with no trouble, at the least in certain contexts.’ It’s the ‘crawl-walk-run’ scenario, and we’re all now somewhere in the center of that evolution, so agencies can beginning to event what can occur as this expertise starts to expand and evolve. What we present is basically like a ‘starter kit’ so groups can get a head delivery on being capable of undertake the capabilities and achieve gains from this mysterious component called unified communications and collaboration.”

Tighter Integration with business approaches

Logicalis is a global company of excessive-efficiency IT integration options – providing cozy, converged computing and communications infrastructure and services. Ron Temske, vp of Cisco (news - Alert) solutions at Logicalis, says, “We work in the UC space, primarily with Cisco, so most of my statements may be a bit specific to their items. We’ve carried out somewhat somewhat with presence. With most of our shoppers, presence is basically a simple ‘Are you on the cellphone and at your desk?’ sort of device these days. consumers are nevertheless of their early phases with this, but they’re intrigued by using it. obviously, we haven absolutely explored all the capabilities and percentages of UC and presence. It’s very a lot in its infancy. In linked areas, you’re seeing the mixing between speedy messaging voicemail, e mail, collaboration, and its becoming greater seamless to, say, cease IM-ing each and every different and click to name each and every different, and things like that.”

“Presence becomes greater pleasing when it will possibly comprise many sources of information into identifying presence reputation, because then it becomes extra beneficial,” says Temske. “it might probably additionally turn into somewhat scary. We’ve heard customers say it will be extraordinary if they might extend presence from their wireless carriers back to their system such that in case you’re at your desk and also you forgot to ahead your calls, the sytem is aware of that your mobile phone is in a car doing fifty five miles per hour down the freeway, so it’s either been stolen or you’re now not in your workplace. Our shoppers additionally ask us when they’ll have provider-federated presence.”

“We’ve seen now not just lots of integration amongst what I call UC purposes but additionally tighter integration with line-of-company purposes,” says Temske. “The name center became the first wave of that, with very basic display pops and the capability to transfer information. but now people need their whole CRM system built-in. An account manager can also need click on-to-name out of Siebel and even just Act. We’re seeing a enormously elevated demand for that. Many new applied sciences go through this section. When phones appeared that might run purposes, you naturally noticed lots of people writing mobile purposes that had no true cause to be there. there have been there as a result of they may be, no longer because they should still be. We’ve long past past that craze and individuals are asking how they could better leverage the mixed capabilities, where the goal isn’t just to run an utility on my telephone but to seamlessly share information and assistance from my company applications and anything gadgets i'll use.”

Let’s social gathering

NEC Unified solutions helps agencies unify their business communications via resourceful software, functions, construction tools, and functions. Paul Lopez, normal supervisor of advertising and marketing and services at NEC (news - Alert) Unified solutions, says, “Presence has existed for quite a while. We’ve had it in touch core items. a customary use case is when a person calls in and an agent should investigate or see if some expert is attainable to take the call or conference a person in. those basic aspects have been available for a while and only in the near past is presence now getting greater prominence from an IP standpoint, such as in IP telephony options. We see it has a foundational building block to get other advantages. Presence in and of itself is just a utility. It’s not an conclusion-all be-all. The actual utility comes with what you assemble on excellent of it.”

“What we see now with presence is the means to deliver more effective communique capabilities on the computer and at the conclusion-person stage, whether they’re cell or at a computer,” says Lopez. “So all of our items are presence-enabled, and all of our software that we’ve brought is presence-enabled. That contains everything from our cellular customer that runs in a variety of PDAs to our gentle customer that runs on the laptop, which we name our Unified client, in addition to products which are shrink-wrapped in a complete solution for SMBs. as an example, we’ve had a lot of success currently with a UC for company answer. It’s a extremely nice finished package that includes everything from a contact middle, conferencing, unified messaging, unified communications, multi function shrink-wrapped container solution. For small corporations, it’s been a real plus. They no longer ought to be troubled about configuring active listing and presence and extensive administration equipment, like a bigger enterprise would do.”

Lopez continues, “When considering presence, you have to ask yourself, ‘Do I really need to understand the finite, granular presence of every person in the business?’ as an instance, in case you and i work at the equal enterprise and also you take a enterprise shuttle and you’re out of the state or nation, maybe I simply should understand that you’re out of the workplace. Do I deserve to recognize that you’re in Japan and in a specific venue? doubtless now not. for those who’re designing your community and your solution, you should believe the have an effect on of presence in a network environment, and how many hits might be taken with the aid of an SQL server, active directory, and all of the commercial enterprise purposes that are running to retain and entry the presence popularity database.”

“At NEC we’ve included a bit greater more desirable presence skill versus every other solutions,” says Lopez. “for example, we do have the means offer some further layers of presence within our cellular or unified customer. if you have a PDA gadget with our cellular customer put in and you go away your computer, taking your PDA with you, our device is aware of that you’re no longer at your desk or desktop, but you’re accessible by means of your PDA, and that has definite aspects and capabilities similar to immediate messaging or voice or anything to permit communications. Single quantity reach is one more tremendous feature that has attracted many of our consumers. It’s rather beneficial. as an instance, in a health care atmosphere, the place a doctor turned into going to call lower back a affected person to check on surgery, they’re calling after hours, and they’re on their cellular telephone. They don’t always desire their cellphone number to appear on a Caller identification machine at the affected person’s home, so via presence and our mobile customer and gateway solution, what comes via when the name is made is basically an extension on the commercial enterprise telephony gadget. We recognize the doctor’s presence and he can set his status along with his PDA, and there's a stage of privateness that we are able to present to that category of person.”

Nortel’s Wes Durow, vice chairman, international commercial enterprise advertising and marketing and strategy, says, “until lately there changed into considerable funding in tools for discrete-productiveness beneficial properties, tools such as e mail and mobile phones, voicemail and unified messaging and company system applications, all constructed by using Oracle and SAP and others. They’re all splendid for my part, but we’re now in an atmosphere where it’s just about like there’s a cyber Kudzu around our enterprises and their enterprise approaches, so today you’re in a lots distinct ambiance. in any case, diverse studies point out that 70 p.c of our outgoing voice calls end up in a message box. Then consider the number of inboxes you have: a voicemail inbox, a cellphone inbox, and a personal email inbox. and you have to deal with middleware and HR solutions to ok someone’s carry, vacation or earnings, and purchasing on-line solutions the place you go in and approve someone’s buy orders. equal issue with IT – who has remote access authorization capability? Who receives a pc and where is it moved. So, on typical, you've got about seven distinctive kinds of inboxes that you’re managing all the way through the day. We’re including latency to the equipment, which we are looking to in the reduction of. That’s the place had been see the force and the hobby in the first phase of UC at the computer degree, after which the evolution of that into the middleware utility level and business technique software stage.”

“Fred Weber is an 800-grownup building and substances deliver company out of St. Louis, Missouri,” says Durow. “They realized that they had finite components, it phrases of labor and a considerable number of raw substances, however they desired to be in a position to interface with the entire substances suppliers to make sure that, when they’re on-web site, they don’t desire worker's on-web site getting paid for not doing any work. on the equal time they don’t are looking to have materials on-web site with no employees there, because then they should do issues like run and get a 2d concrete truck since the first one is beginning to harden. So their complete enterprise case about why to circulate to UC in basic terms had to do with useful resource optimization, enabling presence, and making certain they’re obtained the correct people and the correct job set on the right time with the correct guidance to be helpful. Weber’s total enterprise case is constructed on this.”

“Heathcare has also been extremely energetic in this area,” says Durow.

protection First

As more and more disparate devices and networks develop into “unified”, security and coverage choices turn into extraordinarily crucial for any business desperate to harness the expertise of UC and presence. enterprises need to be able to become aware of unauthorized VoIP gadget use, prevent service disruptions and eavesdropping, and computer screen for brand spanking new threats against the converged infrastructure, while at the same time ensuring reliability and pleasant of provider.

for example, Enterasys Networks, an organization heavily into community safety, and whose convergence, connectivity and compliance solutions convey company-oriented, policy-based visibility and handle of individual user and application priority and security to companies global, currently introduced that it turned into the primary networking business to comprehensive certification for ShoreTel’s know-how partner software. ShoreTel is a massive company of pure IP UC solutions. ShoreTel allows any-sized enterprise to seamlessly combine all of their voice, records and messaging with their business procedures.

as opposed to approaching VoIP safety in a piecemeal, slapdash fashion, Enterasys recommends an intelligent, computerized and integrated approach to permit and at ease wired and instant VoIP communications. The Enterasys comfortable Open Convergence solution can experience and instantly respond to safety threats against the IP telephony infrastructure, enforce community access handle guidelines, and conform to rules for monitoring and safeguard such as CALEA and E911 in the U.S. superior Enterasys Dragon protection purposes have the potential to realize specific threats in opposition t the voice infrastructure by using a strong set of VoIP attack signatures that encompass decoders for H.323, H.245, SIP and Media Gateway control Protocol (MGCP). as soon as threats towards voice services are detected, NetSight computerized protection management can find the actual source of the risk and take applicable action.

The Enterasys Matrix and SecureStack switches are network switching and routing contraptions which immediately discover, classify and prioritize ShoreTel UC programs and site visitors. Embedded safety, priority and bandwidth control is provided for every user, device and utility whereas keeping performance. The Enterasys open architecture interoperates with the existing infrastructure.

Like Two Peas in a Pod

Unified communications and presence are two inseparable objects as a way to dominate the business world, and maybe even your very own lifestyle. extra effective communications are good for everybody – until they occur in wee hours of the morning, of direction.

Richard Grigonis is government Editor of TMC (news - Alert)’s IP Communications community. To read extra of Richard’s articles, please consult with his columnist web page.

Edited through Erik Linask

(supply: http://www.tmcnet.com/channels/call-core-utility/articles/42809-inseparable-presence-unified-communications.htm)




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The Very Best Exploration Games of All Time | killexams.com real questions and Pass4sure dumps

Note: This article was updated in October of 2018.

Exploration is one of the main facets of video games, especially modern ones, that take games well beyond the territory of Pong and Super Mario Bros. and invite them to immerse themselves within worlds fantastic.

Well beyond completing mission objectives and furthering the storyline, games that offer exploration as a choice allow players to fully immerse themselves within these virtual environments, discovering facets of the game that otherwise elude players who’d choose instead to breeze through the story for the sake of finishing the game.

To incentivize exploration, developers hide quests, bits of collectibles, as well as easter eggs for adventurers to find and discover, providing them with countless memories to call their own.

In this list, we cover some of the medium’s best exploration games of all time. If you think we left anything out, feel free to chime in the comments below, and be sure to tell us what you’re looking forward to playing–what game you’re interested in exploring.

#19 Far Cry 5

The fifth main title within the franchise, Far Cry 5, takes place within the United States of America in a fictional Montana area known as Hope County.

Within the narrative, Far Cry 5 pins players against Joseph Seed, a leader of a cult who has forced his way into controlling Hope County. As more innocent civilians become trapped and forced into submission under Joseph Seed’s rule, only a handful of resistance stands in his way.

Just as before, players can expect the title to deliver as a first-person shooter in an open world environment which can be explored either on foot or through vehicles. However, the campaign can be experienced both as a single player narrative or through cooperative multiplayer.

#18 Final Fantasy XV

Final Fantasy XV is an action role-playing video game and the fifteenth main installment to the Final Fantasy franchise. Overall the story of Final Fantasy XV will center between two empires that have declared war, Lucis, and Nifheim, though after Nifheim successfully captures the kingdom’s crystal of Lucis, a group of friend’s sets out to regain it.

Players take control of Noctis, prince of Lucis, who teams up with his fellow friends on a grand journey against a massive empire force. The game is also set in an open world environment with available quests and collectibles to gather. Gamers are encouraged to explore the wide-open environments likewise, there was much to discover in the game’s open world as you completed the lengthy campaign.

#17 STALKER: Shadow of Chernobyl

The atmosphere of STALKER is so thick you could cut it with a knife. And the atmosphere is what defines STALKER.

It’s a first person, survival-horror game set within the radioactive wasteland of Chernobyl, where men known as Stalkers eke out a dangerous living by retrieving strange, reality-defying artifacts. They aren’t alone in the wasteland, which is haunted by mutant horrors and an assortment of nightmarish creatures.

This open-ended setting allows for players to perform a myriad of objectives for the wasteland’s human inhabitants while unraveling the mystery of Chernobyl.

#16 Yakuza 6: The Song of Life

For those familiar with the Yakuza series, the seventh main installment of the series, Yakuza 6: The Song of Life which will pick back up the narrative storyline players have been following over the years.

The game has already released in Japan where it has received a positive reception. Gamers can still expect a brawler type gameplay set in an open world environment. Much like previous installments, players will have the ability to level up various skills and abilities to use against other yakuza thugs in battle.

As for the narrative, players will step into the shoes of Kazuma Kiryu once again who is on a mission to learn what has happened to Haruka after being locked away for three years. The game does feature an open world city for players to explore and as you progress you’ll gather exp to use towards making upgrades such as agility or strength along with unlocking new skills.

#15 Assassin’s Creed: Odyssey

Assassin’s Creed Odyssey is set in 431 BCE where players will have the choice of being a mercenary that fights for Athens and the Delian League or the Peloponnesian League led by Sparta. Either way, players will be a descendant of Spartan King Leonidas I during the Peloponnesian War.

Much like the previous Assassin’s Creed installments, Assassin’s Creed Odyssey will feature a modern day protagonist as well. Ubisoft will be reintroducing players to Layla Hassan who was present during Assassin’s Creed Origins.

There will also be an RPG progression system included in the game as well where players can adjust their character skills and attributes. Likewise, with a branching dialogue system, your narrative journey may offer a unique ending thus giving players an incentive in going back and replaying the game.

#14 Far Cry 4

Much like the previous installment, Far Cry 4 makes our list. This time around, players take on the role of Ajay Ghale, a young Kyrati-American who travels back to his home country of Kyrat, a fictional Himalayan country.

During his travel, Ajay finds that this home country has been caught in a civil war that is controlled by a tyrant king, Pagan Min. A large portion of the game allows players to freely explore the Himalayan country and the wildlife that dwells within it. Furthermore, because the game has a few different storyline branches, gamers will likely replay the title a few times, offering a chance to explore a bit more of the world than before.

#13 Spider-Man

Spider-Man was developed by Insomniac Games who are previously known for their Ratchet & Clank and Resistance video game franchises. Their latest title breathes some new life into the Spider-Man story as this video game title will not be linked to any past comic books or cinematic movies.

Furthermore, the game doesn’t offer the normal origin story of Spider-Man, instead, the video game will be focused around Peter Parker, eight years after he has established the role of being the famed hero. From what we know so far, this is an open-world title where the narrative will follow Peter Parker graduating college while keeping up as protector of New York City.

The video game will also give players the ability to go through the narrative as not only Spider-Man but as the civilian Peter Parker character as well. From what we know from so far through trailers released, Spider-Man’s main antagonist will be Mister Negative, who turns out to be Martin Li, one of New York’s prominent philanthropist and owner of the F.E.A.S.T. shelters that Peter’s Aunt May is employed.

Outside of the campaign, players can freely explore New York City where crimes and collectibles will pop up throughout the area in need of Spider-Man’s attention.

#12 Fallout 4

The Fallout franchise has hit this list several times in the past and now with its most recent installment available in the marketplace, we can’t help but add Fallout 4. If you’re a fan of the franchise then it’s likely you’ve already picked up the latest release.

However, if you’re completely new to the franchise, Fallout 4 still marks as a great first entry to the series. Set during the events of a nuclear war, players manage to escape into a vault, only to awaken hundreds of years into the future. What’s left of your world is nothing more than decay and outsiders trying to make it by in this new world.

Each installment to the Fallout franchise manages to bring out an incredible wasteland to explore and Fallout 4 is no exception to that trend. You’ll come across old ruins, new structures, and a fleshed out cast of characters to meet along your journey.

#11 Far Cry 3

Far Cry 3 has drawn comparisons to The Elder Scrolls: Skyrim in its encouragement of exploration, hunting, and crafting, the open world experience is actually quite different between the two.

While Skyrim allows the player to take the entire map at their own pace, regardless of their participation in the main quest line, Far Cry 3 is designed for the player to balance their exploring with making progress in the game. However, you will find pockets of time to wander about as you please, and indulging in what Rook Island has to offer will greatly aid you in your quests.

Far Cry 3 is proof that first-person shooters can offer more in the way of exploration and world-creation beyond shooting people in corridors.

#10 Dragon Age: Inquisition

The third major installment to the Dragon Age franchise, Dragon Age: Inquisition is an action role-playing video game where players take on the role of an Inquisitor who is on a grand journey to deal with the civil unrest within the continent of Thedas.

While developers have set the game to be on the same continent of the past two installments, exploration for Dragon Age: Inquisition is rather massive in comparison. For instance, it’s been noted that the game features a map that is already five times larger than the setting of the first installment of the series. With all that said, you’ll want to set aside some time to really dive into the video game.

As mentioned, The latest entry in the long-standing series of role-playing games from BioWare offers wide open environments, unlike the two previous games. Players have the ability to explore the map, uncovering new quests and discovering hidden treasures with the newly added ‘ping’ button that lets you investigate your surroundings.

#9 Horizon Zero Dawn

Horizon Zero Dawn is the first IP developed by Guerrilla Games since their release of Killzone in 2004. This is an action role-playing video game title that is set a thousand years into the future.

Mankind has mysteriously fallen, with cities only a shell of a once thriving society. Now only small tribal groups remain where giant mechanical beasts roam the world freely in charge. The plot revolves around a female hunter named Aloy who sets out on a journey to explore the open world, meet with other tribes, and potentially learn of the reason mankind fell to being with.

#8 Monster Hunter: World

The Monster Hunter franchise is consistently growing and with each new installment, a number of new gamers explore the monster-filled worlds development studio Capcom has crafted. Monster Hunter: World will mark as the fifth main installment to the franchise and as you can expect, there will be a number of notable updates.

For instance, Capcom has placed larger maps, a more seamless experience between zones and what’s a Monster Hunter video game without the ability to hunt with friends? Outside of the offline campaign, the game will allow a four-player online co-op opportunity.

This might not be directly an open world video game but players will still find a rather large environment to explore. Also if you’re a newcomer to the series then this will still mark as a great title to jump on but you will find that the gameplay can still be a bit advanced. Luckily the community is very active supporting other players with helpful guides and tricks to make your first hunt a successful one.

#7 Metroid Series

The Metroid series has been around for decades and continues to gather new fans while inspiring other developers when it comes to the creation of their own IP. You may have heard of the term Metroidvania tossed around for certain video game titles and its used to describe similarities from the Metroid series.

Metroid has a heavy emphasis on exploration. You’ll find yourself gathering a certain item or power that will allow players to access certain areas that were previously unreachable or locked away.

#6 The Legend of Zelda: Breath of the Wild

The Legend of Zelda: Breath of the Wild is the nineteenth main installment to The Legend of Zelda franchise. This time around, players will be placed in a large open-world environment with the ability to play through the game’s dungeons in any order.

Within The Legend of Zelda: Breath of the Wild, players will take on the role of Link after he awakens from a deep slumber that lasted a hundred years. A mysterious voice alerts link to reach a ruined Kingdom known as Hyrule where he will learn of Calamity Ganon, the antagonist who had previously destroyed Hyrule, though, during the process, he had trapped himself within the buried kingdom.

#5 The Witcher 3

Fans of western RPGs will no doubt have played at least one of the Witcher games. This series of Polish games based on the works of Andrzej Sapkowski has gained a lot of fans over the years, mainly thanks to its complex world and stories, incredible graphics and deep gameplay systems.

The third and final installment in the series sees a much older Geralt of Rivia – one of the titular Witchers – dealing with the invasion of the Northern Kingdom by the Nilfgaard Empire and the otherworldly threat of the Wild Hunt, spectral riders who’ve plagued humankind for ages. Offering a massive open world, hours upon hours of story content and side quests, tons of NPCs to interact with and monsters to hunt, a living economy that adapts to different locations and events and improved gameplay, The Witcher 3: Wild Hunt is looking like a worthy conclusion of the series.

#4 Minecraft

Minecraft is ultimately our number one pick for the best open world video game ever made based on the simple fact that the world in which it takes place is that of our own creation.

It offers players the ability to build kingdoms, go on adventures, and craft narratives that far transcend anything created by a game developer. The world of Minecraft is a sandbox, and it’s ours to play in and to do as we like.

The game is what you make of it.

#3 The Elder Scrolls V: Skyrim

Skyrim is the fifth game in Bethesda’s ever-popular series of role-playing games. Like its predecessors, Skyrim takes place in an open environment in which we’re given leave to explore the world as we see fit.

While the world of Skyrim is charming and consistently engaging,  it doesn’t simply tell us a story—it offers us instead a chance to weave our very own tale.

Skyrim is interactive art at its finest.

#2 Red Dead Redemption

Red Dead Redemption is the Old West made anew with the fiction of Rockstar Games, and it’s every bit as bleak and unforgiving as it was back in the olden days.

It is within this unforgiving land that a man, John Marston, seeks redemption—not only for his life but for his soul. And it is only within this land that such redemption is possible.

Needless to say, the game’s atmosphere is second to none, and it is host not only to John Marston’s story and those of his counterparts but to the greater battle between the old and the new—the stolid Old West and the march of Progress.

Players will likely enjoy the exploration that ranges from the game’s Texas analog to the Mexican desert across the border. All along the way, there’s “Strangers” to encounter, all of whom have their own strange tales to share with the player.

#1 Grand Theft Auto V

Much like Red Dead Redemption, there is plenty to explore and discover in the city of Los Santos and its surrounding environments. The city itself is filled to the brim with strange people, whose lives and stories are intertwined with that of the city.

This is by far one of the most lived-in feeling cities from the Grand Theft Auto franchise and even if you’re completely done with the campaign and side quests that present themselves to the player, Rockstar has a whole different side of the world for gamers to enjoy. Thanks to Grand Theft Auto Online, players have even more options and features to enjoy with the game all while combining players from all around the world to wreak havoc on Los Santos together.


Nuance’s Dragon Drive! Messaging Powers Text Message Dictation in the New Audi A3 | killexams.com real questions and Pass4sure dumps

BURLINGTON, Mass.--(BUSINESS WIRE)--Nuance Communications Inc. (NASDAQ: NUAN) today announced that its automotive-grade Dragon Drive! Messaging service for the connected car is powering the text message dictation in the new Audi A3, creating a hands-free messaging experience. With Audi connect Messaging, drivers can simply use their voice to dictate and send text messages while driving, as well as hear incoming text or e-mail messages.

The Audi A3 deeply integrates Dragon Drive! Messaging as part of the in-car user interface. Drivers simply connect their phone via Bluetooth or insert their SIM card into the MMI Navigation plus to quickly and easily dictate and send text messages without having to take their hands off of the wheel. For example, just say “Dictate text message to John Smith” to quickly access the contact from a mobile address book, and then speak the message, “I am stuck in traffic and will be late for the meeting. Start without me.” The message is read to the driver, and from there they can continue dictating, edit or send the message using simple voice commands. Nuance’s natural, humanlike text-to-speech capabilities also read out incoming text and email messages, keeping Audi drivers connected to friends and family from anywhere.

“The in-car experience is quickly evolving from simply keeping drivers entertained to keeping them connected and productive in safer, smarter ways,” said Arnd Weil, vice president and general manager, automotive, Nuance Mobile. “Dragon Drive! Messaging’s flexible and customizable architecture enables world-leading automotive brands like Audi to deeply integrate powerful voice capabilities as part of their unique in-car experience, without compromising quality or adding dangerous distractions.”

Audi also integrates Nuance’s voice command and control as part of Audi’s voice user interface, letting drivers speak voice commands to search and access contacts and make calls on their phone, select Audi connect services and one-shot voice commands to input navigation address information.

Availability

Audi connect Messaging with dictation capabilities will be available with Audi connect and MMI Navigation plus on the new Audi A3 shipping at the end of 2012 in Europe and will initially support several European languages.

Dragon Drive! is Nuance’s automotive-grade platform that fully harnesses Nuance’s deep expertise and research in natural language understanding voice technologies to deliver connected and embedded services like Dragon Drive! Messaging. The result is an in-car experience that lets drivers engage hands-free, ultimately minimizing driver distraction.

Dragon Drive! is a part of Nuance’s broad Dragon portfolio, including Dragon NaturallySpeaking, Dragon Dictate for Mac, Dragon Dictation, Dragon Go!, Dragon TV and Dragon ID, all humanizing the way people engage their phones, tablets, TVs, cars and computers – just by using their voice. To learn more about all that Nuance’s Dragon portfolio has to offer, visit www.nuance.com and www.nuancemobilelife.com.

About Nuance Communications, Inc.

Nuance Communications, Inc. (NASDAQ: NUAN) is a leading provider of voice and language solutions for businesses and consumers around the world. Its technologies, applications and services make the user experience more compelling by transforming the way people interact with devices and systems. Every day, millions of users and thousands of businesses experience Nuance’s proven applications. For more information, please visit www.nuance.com.

Nuance and the Nuance logo are trademarks or registered trademarks of Nuance Communications, Inc. or its subsidiaries in the United States of America and/or other countries. All other company names or product names may be the trademarks of their respective owners.

The statements in this press release relating to future plans or future events or service, are forward-looking statements which are subject to specific risks and uncertainties. These could involve particular market trends, competition factors and other risks described in the documents submitted to the US Securities and Exchange Commission. The actual results, events and services may vary significantly from the forecasts. The reader is warned not to rely on these forward- looking statements without reservation, since these are simply reflections of the current situation.


Polymer Science and Engineering - How and Where AFM is Applicable | killexams.com real questions and Pass4sure dumps

The atomic force microscope is a sophisticated instrument which helps delineate the characteristics of polymers by revealing physical properties and mechanical behavior at nanoscale, as well as providing images. This article discusses the advanced features and benefits of Asylum Research CypherTM and MFP-3DTM AFMs in this field.

Polymers are useful in a host of applications. Their properties can be tuned and may be customized to suit different uses. Moreover, they are often less costly, sturdier and more environmentally friendly than other materials. In order to produce and bring into use a new polymer, the structure, processing, characteristics and performance must all be understood. This is achievable at micro- or molecular level if the data acquired is of this resolution.

Figure 1 shows AFM usage in analyzing the basic principles underlying polymers, while Figure 2 shows its employment in engineering a particular solution of a polymer. The point is that AFM plays a vital role in assessing polymers at these small length scales [1-4]. The high spatial resolution brings polymer morphology into view at resolutions below micrometers or even nanometers. However, much more data can be obtained using AFMs, such as molecular forces, mechanical, thermal and electrical mapping, and finding the effects of heat or solvents in realistic situations.

Morphology of PS-PEP diblock copolymer film – Tapping mode phase image of a polystyrene-block-poly(ethylenealt-propylene) (PS-PEP) film on a silicon wafer. The darker region on the left side with lower phase corresponds to the high side of a 16 nm step in the wafer. In this region and the darker curved region on the right, the film forms a PS wetting layer. In the lighter region with higher phase, the film contains a single layer of spherical PEP microdomains. Several vertical rows of aligned microdomains are seen on the low side of the step. Diblock copolymers can self assemble into complex periodic structures, a property that has attracted interest for their use as templates in nanolithography. Understanding how film thickness and step height affect domain location and orientation aids in developing block copolymer templates. Imaged with the MFP-3D AFM; scan width 2 μm, Z (phase) scale 10°. Adapted from Ref. 5.

Figure 1: Morphology of PS-PEP diblock copolymer film – Tapping mode phase image of a polystyrene-block-poly(ethylenealt-propylene) (PS-PEP) film on a silicon wafer. The darker region on the left side with lower phase corresponds to the high side of a 16 nm step in the wafer. In this region and the darker curved region on the right, the film forms a PS wetting layer. In the lighter region with higher phase, the film contains a single layer of spherical PEP microdomains. Several vertical rows of aligned microdomains are seen on the low side of the step. Diblock copolymers can self assemble into complex periodic structures, a property that has attracted interest for their use as templates in nanolithography. Understanding how film thickness and step height affect domain location and orientation aids in developing block copolymer templates. Imaged with the MFP-3D AFM; scan width 2 μm, Z (phase) scale 10°. Adapted from Ref. 5.

Distribution of components in EVA-EPP-carbon black blends – Images of tapping mode topography (left) and phase (right) of semiconducting polymer blends. The blends contained two polyolefin copolymers, poly(ethylene vinyl acetate) (EVA) and ethylene-propylene copolymer (EPP), mixed with carbon black (CB). The images correspond to blends with 10 wt % (top) and 30 wt % (bottom) EPP. Carbon black is an economical filler used in many practical applications to create electrically conducting polymers. However, addition of CB can significantly affect blend qualities such as viscosity. The use of two copolymers achieved a balance between performance (electrical volume resistivity) and processing (melt flow rate). The phase images clearly differentiate individual blend components, allowing the effect of component distribution on conductivity to be studied. Imaged with the MFP-3D AFM, scan size 20 μm. For more information see Ref. 6.

Figure 2: Distribution of components in EVA-EPP-carbon black blends – Images of tapping mode topography (left) and phase (right) of semiconducting polymer blends. The blends contained two polyolefin copolymers, poly(ethylene vinyl acetate) (EVA) and ethylene-propylene copolymer (EPP), mixed with carbon black (CB). The images correspond to blends with 10 wt % (top) and 30 wt % (bottom) EPP. Carbon black is an economical filler used in many practical applications to create electrically conducting polymers. However, addition of CB can significantly affect blend qualities such as viscosity. The use of two copolymers achieved a balance between performance (electrical volume resistivity) and processing (melt flow rate). The phase images clearly differentiate individual blend components, allowing the effect of component distribution on conductivity to be studied. Imaged with the MFP-3D AFM, scan size 20 μm. For more information see Ref. 6.

Investigating Morphology and Structure

Polymer structures change at different scales of length. These smaller scale structures include a brush configuration, and if single molecules are visualized, chain packing; for crystalline polymers, lamellar formations; and with block or graft copolymers, microphase separation. Features visible on larger scales include pores or fillers, and for blends of polymers, interfacial phases. Effects of processing like etching, heat or strain are also visible on the surface roughness or finish. The study of nanoparticles, nanofibers and nanodevices made of polymer includes statistical analysis of both individual components and the whole assembly’s shape and size.

The AFM allows the structure to be visualized via nanoscale topography of the surface, typically in tapping mode. This mode yields images with excellent spatial resolution, up to molecular and atomic structure, as Figure 3 reveals. The small area in contact between the tip and the sample is responsible for the high resolution. This in turn is achieved by using ultrasharp tipped probes, in addition to the tapping mode which results in very gentle sideways and vertical forces between the tip and the sample.

As Figure 4 shows, AFM imaging has recently become much faster with the emergence of newer AFMs, such as the Cypher AFMs from Asylum Research. This is due to the use of small cantilevers. Not only do smaller cantilevers have higher resonant frequencies, they are also able to provide improved resolution and control for very small forces in the subpiconewton range, which is extremely crucial when investigating polymers which are delicate and easily undergo deformation.

Molecular and crystalline structure of rubrene – Tapping mode topography images of crystalline rubrene imaged with the Cypher S AFM. Rubrene is a polycyclic aromatic hydrocarbon used as an organic semiconductor in organic light emitting diodes. The main color image with scan size 5 μm shows single steps of the crystalline lattice. The inset black-and-white image reveals molecular-level structure, highlighting the superb spatial resolution of Cypher AFMs, even in air. Scan size 20 nm. Sample courtesy of Rutgers University.

Figure 3: Molecular and crystalline structure of rubrene – Tapping mode topography images of crystalline rubrene imaged with the Cypher S AFM. Rubrene is a polycyclic aromatic hydrocarbon used as an organic semiconductor in organic light emitting diodes. The main color image with scan size 5 μm shows single steps of the crystalline lattice. The inset black-and-white image reveals molecular-level structure, highlighting the superb spatial resolution of Cypher AFMs, even in air. Scan size 20 nm. Sample courtesy of Rutgers University.

PHB/V spherulite crystallization – Tapping mode phase images of a polyhydroxybutyrate-co-valerate (PHB/V) spherulite crystallizing at room temperature over a period of three minutes. Scan size 1.5 μm. The scan rate of 40 Hz, or approximately 10 seconds per frame, allows clear visualization of the crystallization process. Imaged with the Cypher AFM. Sample courtesy of the University of Sheffield.

Figure 4: PHB/V spherulite crystallization – Tapping mode phase images of a polyhydroxybutyrate-co-valerate (PHB/V) spherulite crystallizing at room temperature over a period of three minutes. Scan size 1.5 μm. The scan rate of 40 Hz, or approximately 10 seconds per frame, allows clear visualization of the crystallization process. Imaged with the Cypher AFM. Sample courtesy of the University of Sheffield.

Using Asylum AFMs for Topographic Imaging
  • All Asylum AFMs use closed-loop scanning which has the advantage of repeatable and precise scanning motions due to the use of position sensors. As a result, image distortions are avoided, with very precise offsets, while specific scan areas are zoomed in to. The Cypher 5 and ES, as well as the MFP-3D InfinityTM all have the most advanced sensors with remarkably low noise, down to 35 pm and 60 pm in the Z, and X and Y, axes respectively.
  • The Cypher family AFMs use small cantilevers of less than 10 microns length, so that imaging goes faster, and standard line scan rates are up to 10-40 Hz. These also have better resolution and lower noise, and thus the DNA helix and single point atomic defects are now imaged on a routine basis.
  • GetStartedTM is integrated with the MFP-3D Infinity and all Cypher AFMs to automate image parameters. Even before the first tip-sample contact, the parameters are defined automatically using a predictive algorithm. This protects both sample and tip against wear due to non-optimal contact, and also ensures the acquisition of excellent data starting from scan line 1.
  • Measuring Forces and Deformation

    The cantilever used in AFMs is one which is built with extreme force sensitivity, which makes it ideal for the measurement of a range of force magnitudes from piconewtons to micronewtons. This contains most polymer interactions too. There are two common ways to measure force: either single molecules are pulled to analyze the forces at molecular level, or polymeric materials are indented to evaluate their elastic and viscoelastic return following deformation.

    When the single molecule approach is used, one molecule is stretched between the tip of the AFM and the sample surface, and the deflection of the cantilever is measured. Once the spring constant and deflection sensitivity of the cantilever is known, a force vs. distance plot is generated. These force curves provide information about intramolecular forces, like the elasticity of the single chain, or conformational transitions, as well as intermolecular forces, including interactions between polymer and solvent, and surface adhesion and desorption.

    These forces thus act inside or between the molecules. One case of force spectroscopy measurement is shown in Figure 5, using poly-L-lysine molecules during their desorption from a hydrophobic surface.

    The other method uses measurements of the deflection produced in the cantilever as the AFM tip indents the sample. Conventionally used cantilevers apply a force that is high enough to cause deformation in the polymers which have modulus ranging from kPa to a few GPa. When a model is used to examine the indentation of the sample by the tip, data is generated on the elastic and viscoelastic characteristics of the sample at nanoscale.

    Asylum AFMs for Measuring Force
  • GetRealTM is integrated into all Asylum AFMs, being a software to calibrate the cantilever spring constant and deflection sensitivity automatically at one click, without having to touch the surface of the sample.
  • All Asylum AFMs have force measurements which are thermally limited and use Z sensors for low noise. This allows measurement of both axes of the force curves with as much sensitivity and accuracy as possible.
  • All Asylum AFMs are programmed to analyze force curves with sophisticated features. Several pre-set indentation models are available, such as Hertz/Sneddon, Johnson-Kendall-Roberts (JKR), Derjaguin-Müller-Toporov (DMT), and Oliver-Pharr. In addition there is a guide to model selection which shows the plasticity index, the ratio of force to adhesion, and Tabor coefficient calculation.  
  • Mapping Nanomechanical Properties

    Polymers must have certain mechanical attributes to suit their varied applications, such as food packaging to flexible electronic devices. Sometimes one or more components with phase separation, or a filler, could be added to enhance the mechanical performance. In most cases they are at nanoscale and thus their mechanical properties must be measured at this spatial resolution.

    Asylum has multiple techniques for nanomechanical studies, from simple methods of quantitation to advanced quantitative techniques. In many situations the two are used to complement each other in a way that informs the observer about the polymer sample.

    The introduction of the tapping mode for phase imaging created much interest in the late nineties. This has led to the emergence of phase imaging as a very useful tool for characterizing polymers, since it can resolve the fine structure of the molecule and distinguish various components of the material.

    Sometimes interpretation of the results becomes difficult because of the influence of the mode of storage and dissipation of elastic energy and viscous energy by the material, respectively, (the loss tangent) in addition to other forces that cause dissipation. Yet phase imaging is still a relatively easy and widespread method of acquiring qualitative data on material properties.

    Another way to obtain a qualitative map of material property changes is the use of bimodal imaging or Dual ACTM which is similar to the tapping mode with phase imaging at bottom, with the difference being the driving of an additional cantilever mode along with the first mode. Topography and phase measurements from the first mode are taken along with amplitude and phase response measurements from the second mode. Again, the interpretation is sometimes complicated, but its use remains valid for acquiring contrast where this is not possible by phase imaging.

    The Asylum NanomechProTM Toolkit lists many methods, among which the unique AM-FM Viscoelastic Mapping Mode is ideal for polymers. Like bimodal imaging, this technique makes use of tapping mode to operate at two cantilever mode frequencies at the same time. The second mode is tracked for its frequency and correlated with the stiffness of the sample.

    The first mode is related to the loss tangent of the sample through its phase and amplitude. The net result is clear quantitative mapping of the elastic storage modulus and the viscoelastic loss modulus, or loss tangent, but with the rapidity expected with the tapping mode and with sample preservation. The large range of applications possible with the AM-FM mode, making it possible to test almost any polymer, is because of the impressive breadth of its measurement range from under 1 MPa to over 100 GPa. One instance where AM-FM mode is used to map a polymer assembled from multiple components is shown in Figure 6.

    Single molecule forces for poly-L-lysine homopolymer – (top) Graphic of force spectroscopy concepts. A single polymer molecule is covalently attached to the AFM tip by a linker (here, polyethylene glycol, PEG). (bottom) Force-distance curve for poly-L-lysine on a hydrophobic self-assembled monolayer (SAM) in water. The force plateau indicates the desorption of a single polymer from the surface. Histograms obtained from multiple force curves provide the average desorption force (inset, top) and detachment length (inset, bottom) Acquired with the MFP-3D AFM. Adapted from Ref. 7.

    Figure 5: Single molecule forces for poly-L-lysine homopolymer – (top) Graphic of force spectroscopy concepts. A single polymer molecule is covalently attached to the AFM tip by a linker (here, polyethylene glycol, PEG). (bottom) Force-distance curve for poly-L-lysine on a hydrophobic self-assembled monolayer (SAM) in water. The force plateau indicates the desorption of a single polymer from the surface. Histograms obtained from multiple force curves provide the average desorption force (inset, top) and detachment length (inset, bottom) Acquired with the MFP-3D AFM. Adapted from Ref. 7.

    Mechanical mapping of a bonded polymer interface – AM-FM Viscoelastic Mapping Mode images and histograms of (left) loss tangent and (right) second mode frequency overlaid on topography for a rubber-epoxy-latex sandwich. Imaged with the Cypher S AFM; scan size 5 μm. Different sample components are clearly distinguished by the AM loss tangent of viscoelastic damping. They are also resolved by the FM frequency, which is proportional to elastic stiffness, despite very similar modulus values for latex (~40 MPa) and rubber (~43 MPa).

    Figure 6: Mechanical mapping of a bonded polymer interface – AM-FM Viscoelastic Mapping Mode images and histograms of (left) loss tangent and (right) second mode frequency overlaid on topography for a rubber-epoxy-latex sandwich. Imaged with the Cypher S AFM; scan size 5 μm. Different sample components are clearly distinguished by the AM loss tangent of viscoelastic damping. They are also resolved by the FM frequency, which is proportional to elastic stiffness, despite very similar modulus values for latex (~40 MPa) and rubber (~43 MPa).

    Modulus mapping of PS-PCL blend – Elastic modulus overlaid on topography for a polystyrene (PS)-polycaprolactone (PCL) blend. Imaged with Fast Force Mapping Mode on the MFP-3D Infinity AFM; scan size 4 μm. The 1024x1024 image size would be impractically slow to obtain with conventional force volume techniques. It provides superb lateral resolution, resolving features as small as approximately 10 nm. As expected from bulk literature values, PS regions (yellow)have higher modulus (approximately 3 GPa) than PCL regions (purple, approximately 350 MPa). The biodegradable nature of polycaprolactone is valuable in development of new bioblend materials.

    Figure 7: Modulus mapping of PS-PCL blend – Elastic modulus overlaid on topography for a polystyrene (PS)-polycaprolactone (PCL) blend. Imaged with Fast Force Mapping Mode on the MFP-3D Infinity AFM; scan size 4 μm. The 1024x1024 image size would be impractically slow to obtain with conventional force volume techniques. It provides superb lateral resolution, resolving features as small as approximately 10 nm. As expected from bulk literature values, PS regions (yellow)have higher modulus (approximately 3 GPa) than PCL regions (purple, approximately 350 MPa). The biodegradable nature of polycaprolactone is valuable in development of new bioblend materials.

    Force curves are one established method of elastic modulus measurement. It is suitable for when point measurements are in view, but mapping using this technique is so slow as to be non-feasible. Typically, a 256x256 pixel array is acquired in more than 18 hours, at 1 second per pixel.

    This issue is resolved by the Fast Force Mapping Mode from Asylum, integrated into the MFP-3D Infinity AFM, which has force curve acquisition rates of up to 300 Hz, thus taking below 10 minutes to acquire a 256x256 pixel image of complete deflection vs Z sensor force curves. At this speed there are still no curves found missing nor is there any invisible manipulation of the data. Figure 7 shows how Fast Force Mapping is carried out on a phase-separated polymer blend.

    Another special method pioneered by Asylum is the Contact Resonance Viscoelastic Mapping Mode, used to measure elastic storage modulus as well as viscoelastic loss modulus on polymers with relatively high stiffness, modulus of 1 GPa or more.

    This mode takes advantage of the high sensitivity of the cantilever resonance to any small variations in the mechanical characteristics of the sample after bringing the tip in contact. In common with all these above-mentioned techniques, Contact Resonance can be used either for rapid qualitative mapping, employing the least possible calibration, or for accurate quantitative results after calibrating against a material whose properties are known.

    Asylum AFMs for Mapping Nanomechanical Properties
  • Many techniques are described in the Asylum NanomechPro Toolkit in order to help select the best technique for each application, thus comparing the results obtained using several different techniques.
  • Both AM-FM and Contact Resonance modes assess the viscoelastic response of the sample, that is, the loss modulus or the loss tangent. They also look at its storage modulus or elastic response. This is important to know in a variety of situations which require impact resistance or toughness, which are heavily affected by the material’s viscous properties.
  • The Cypher AFM family uses small cantilevers with the AM-FM Viscoelastic Mapping Mode to perform quantitative mapping of the nanomechanical properties of the sample much quicker than is possible using any other method.
  • The NanoRackTM Stretch Stage is brought into use in some situations requiring the measurement of materials which are under tensile strain, with the MFP-3D AFM series.
  • Measuring Thermal Properties

    Many polymers show very significant changes in properties as the temperature increases. It is important to understand glass transition temperatures and similar characteristics in order to gain a deeper insight into molecular motion. This would enable the evaluation of properties which are critical to their performance such as toughness and impact resistance, and to understand how they are affected by processing or by high temperatures in their operating surroundings.

    When AFM measurements are taken at varying temperatures, they provide data on many processes like crystallization, melting, glass transitions and sub-glass transitions. The use of sample heating stages ensures that temperatures can be varied with strict control over the range to be studied for polymer transitions. Figure 8 illustrates how modulus in polyethylene terephthalate varies with temperature, this being a thermoplastic material. Figure 9 reveals the changes in morphology of a microparticle with shape memory as it undergoes heating.

    In addition to assessing the changes in form and properties in relation to the temperature, there are also ways to directly analyze heat properties at nanoscale. One is scanning thermal microscopy (SThM), which uses a custom cantilever specially designed to make contact with the sample while monitoring the changes in temperature caused by a local heat source. As it measures the local surface temperature of the sample, image contrast is produced in direct relation to the local conductivity to thermal energy. Figure 10 shows an example of SThM used to image a polymer blend.

    Another thermal imaging method is local thermal analysis (LTA), which uses a probe that is heated locally rather than a local sample surface temperature sensor, to heat a nanoscale volume of the sample. With heating or cooling of the sample, there is expansion or contraction in keeping with its local coefficient of thermal expansion. The cantilever deflection reflects this change, generating deflection-temperature curves.

    These curves are extremely sensitive when it comes to detecting the beginning of a thermal transition in the sample, and can thus differentiate various materials by detecting their melting or glass transition temperatures. The use of this technique in testing a ternary polymer blend is shown in Figure 11.

    Temperature dependence of PET viscoelastic properties – (left) Force curve for polyethylene terephthalate (PET). A 3 second hold segment of constant force was applied between the force loading and unloading cycles. (center) Creep curves of indentation versus time during the force curve hold interval. The curves have been normalized to vary between zero and one, highlighting the increase in relaxation time with temperature. (right) Temperature dependence of instantaneous modulus E1 (pink squares) and long term modulus E2 (black diamonds) obtained by fitting the creep curve to a three-element Maxwell-Voigt model (inset, center). Both E1 and E2 exhibit a dramatic drop in the temperature range between the glass-to-rubber transition temperature Tg ≈ 77 °C and the PET crystallization temperature Tc ≈ 13 5°C due to the film’s semicrystalline nature in this range. Acquired with the MFP-3D AFM and PolyHeater sample stage. Adapted from Ref. 8.

    Figure 8: Temperature dependence of PET viscoelastic properties – (left) Force curve for polyethylene terephthalate (PET). A 3 second hold segment of constant force was applied between the force loading and unloading cycles. (center) Creep curves of indentation versus time during the force curve hold interval. The curves have been normalized to vary between zero and one, highlighting the increase in relaxation time with temperature. (right) Temperature dependence of instantaneous modulus E1 (pink squares) and long term modulus E2 (black diamonds) obtained by fitting the creep curve to a three-element Maxwell-Voigt model (inset, center). Both E1 and E2 exhibit a dramatic drop in the temperature range between the glass-to-rubber transition temperature Tg ≈ 77 °C and the PET crystallization temperature Tc ≈ 13 5°C due to the film’s semicrystalline nature in this range. Acquired with the MFP-3D AFM and PolyHeater sample stage. Adapted from Ref. 8.

    Annealing of shape memory polymer – Tapping mode topography images of a polystyrene (PS) microparticle during annealing. Scan size 12 μm, Z (height) scale 1.4 μm. The PS particle was flattened with a high-temperature, high-pressure nanoimprint lithography (NIL) process and then thinly coated with gold. Imaging began with the particle heated to 80°C. The heater temperature was rapidly increased to 102°C and then increased stepwise, so that it was 106°C after 78 min. and 110°C at 170 min. During annealing the particle diameter decreases and the height increases, recovering the original, pre-NIL spherical shape. A surface wrinkling morphology develops that gives information on recovery dynamics and strain energy release. Applications for micro- and nanoscale polymer particles include drug delivery and electronic packaging; incorporating shape memory effects could lead to many more. Imaged with the MFP-3D AFM. Adapted from Ref. 9.

    Figure 9: Annealing of shape memory polymer – Tapping mode topography images of a polystyrene (PS) microparticle during annealing. Scan size 12 μm, Z (height) scale 1.4 μm. The PS particle was flattened with a high-temperature, high-pressure nanoimprint lithography (NIL) process and then thinly coated with gold. Imaging began with the particle heated to 80°C. The heater temperature was rapidly increased to 102°C and then increased stepwise, so that it was 106°C after 78 min. and 110°C at 170 min. During annealing the particle diameter decreases and the height increases, recovering the original, pre-NIL spherical shape. A surface wrinkling morphology develops that gives information on recovery dynamics and strain energy release. Applications for micro- and nanoscale polymer particles include drug delivery and electronic packaging; incorporating shape memory effects could lead to many more. Imaged with the MFP-3D AFM. Adapted from Ref. 9.

    SThM on PP-PS-PE ternary blend – The sample contained 60% polypropylene (PP), 20% polystyrene (PS), and 20% polyethylene (PE) by weight. In this SThM image, the three components are clearly distinguished, with darker colors corresponding to higher thermal conductivity. As expected from literature values for their thermal conductivity, the oblong regions of PS are brightest (yellow, 0.03 W / m•K), the circular regions of PE are darkest (purple, 0.4 W / m•K), and the surrounding PP matrix is intermediate (orange, 0.12 W / m•K).Imaged with the MFP-3D AFM; scan size 15 μm. Sample courtesy of Dalia Yablon and Andy Tsou, Corporate Strategic Research, ExxonMobil Research and Engineering.

    Figure 10: SThM on PP-PS-PE ternary blend – The sample contained 60% polypropylene (PP), 20% polystyrene (PS), and 20% polyethylene (PE) by weight. In this SThM image, the three components are clearly distinguished, with darker colors corresponding to higher thermal conductivity. As expected from literature values for their thermal conductivity, the oblong regions of PS are brightest (yellow, 0.03 W / m•K), the circular regions of PE are darkest (purple, 0.4 W / m•K), and the surrounding PP matrix is intermediate (orange, 0.12 W / m•K).Imaged with the MFP-3D AFM; scan size 15 μm. Sample courtesy of Dalia Yablon and Andy Tsou, Corporate Strategic Research, ExxonMobil Research and Engineering.

    LTA of PP-PE-PS ternary blend – (top) AM-FM Viscoelastic Mapping Mode image of the same sample used in Figure 10. The brighter colors indicate higher modulus. Scan size 6 μm. The black dots indicate points where LTA measurements were made. (bottom) The LTA measurements are color coded with the points in the image and clearly distinguish the different transition temperatures for PS (blue), PE (green) and PP (red). Sample courtesy of Dalia Yablon and Andy Tsou, Corporate Strategic Research, ExxonMobil Research and Engineering.

    Figure 11: LTA of PP-PE-PS ternary blend – (top) AM-FM Viscoelastic Mapping Mode image of the same sample used in Figure 10. The brighter colors indicate higher modulus. Scan size 6 μm. The black dots indicate points where LTA measurements were made. (bottom) The LTA measurements are color coded with the points in the image and clearly distinguish the different transition temperatures for PS (blue), PE (green) and PP (red). Sample courtesy of Dalia Yablon and Andy Tsou, Corporate Strategic Research, ExxonMobil Research and Engineering.

    Asylum AFMs for Thermal Measurements
  • All MFP-3D AFMs except for OriginTM are compatible for the PolyHeater (from ambient temperatures to 300°C), PolyHeater+ (from ambient temperatures to 400°C), and CoolerHeater (from -30°C to +120°C) sample stages. These operate in harmony with the Environmental Controller to achieve a closed-loop control for the temperature which is fully programmable.
  • Cypher ES AFMs have a Heater (temperatures from ambient to 250°C) and CoolerHeater (0°C to 120°C) sample stages. These accurately regulate temperature without the need for external controllers or other electronic components, or for cooling pumps.
  • All MFP-3D family AFMs use state-of-the-art microfabricated silicon probes with the SThM probe holder to achieve SThM temperature and thermal conductivity measurements with higher resolution than Wollaston-wire probes.
  • The Zither™ Modulated Thermal Analysis Option available with Cypher and MFP-3D family AFMs (except Origin) allows LTA to achieve a better than 20 nm lateral resolution. The use of proprietary calibration and measurement protocols make the results extremely sensitive but prevent the occurrence of artifacts like those produced by thermal drift.
  • Monitoring Dynamic Processes due to Solvent and Thermal Effects

    In an environment that is not at room temperature, the change in morphology and physical properties over time must be understood. When a polymer interacts with a liquid or vapor solvent, the durability and performance of the polymer over the long term can go down. In other applications, the rise in temperature can affect the lifetime or dependability of the device.

    Once the solvent concentration or thermal gradients are controlled, the more advanced AFMs such as the Cypher have fast scan rates to monitor dynamic behavior directly, such as degradation or decomposition, chain and brush ordering, formation of lamellae, crystallization and melting. It is possible to obtain movies showing the mechanical or topographical properties if the frame rate is below one minute. In Figure 12, one such instance is seen where the changes in morphology occur when a melted polymer recrystallizes.

    It is often difficult to operate in tapping mode using solvents or other liquids due to the multiple resonance peaks occurring as a result of mechanical coupling between the tapping piezo and the fluid. This has been countered using different techniques using various actuation platforms. That is, actuation by photothermal, electromagnetic or other forces that brings the multiple peaks down to a few, making it easier to use tapping mode with more stable results.

    Recrystallization of PP – A blend of polystyrene (PS) and polypropylene (PP) was heated to 140°C to melt the syndiotactic PP and then cooled at a constant rate while imaging at one frame per minute. As the sample cools, the continuous PP phase first nucleates and then forms partly ordered, semicrystalline regions. Some of the regions form on top of the PS spherical domains. Imaged with the Cypher ES AFM; scan size 4 μm.

    Figure 12: Recrystallization of PP – A blend of polystyrene (PS) and polypropylene (PP) was heated to 140°C to melt the syndiotactic PP and then cooled at a constant rate while imaging at one frame per minute. As the sample cools, the continuous PP phase first nucleates and then forms partly ordered, semicrystalline regions. Some of the regions form on top of the PS spherical domains. Imaged with the Cypher ES AFM; scan size 4 μm.

    Analyzing Electrical and Functional Behavior

    Polymers have unique characteristics and can be manufactured at low costs, rendering them very appealing for a host of applications like flexible electronics, photovoltaics using organic sources, organic LEDs, MEMS actuators and sensors, and data storage devices. At nanoscale, the electrical and mechanical properties of these materials must be well understood, and this becomes more vital as miniaturization of devices proceeds. One particularly important area is finding the correlation between any local heterogeneities and the bulk performance.

    There are specialized modes of AFM operation to examine the electrical and electromechanical behavior of nanoscale of polymers which have conductive, semiconducting and dielectric properties. Some of these modes are conductive AFM (CAFM), electric force microscopy (EFM), and Kelvin probe force microscopy (KPFM). These yield electrical data on conductivity, surface potential, photocurrents and work function.

    When piezoelectric and ferroelectric polymers are being tested, piezoresponse force microscopy (PFM) is used to analyze electromechanical behavior at nanoscale, such as polarization switching and domain growth. Figure 13 shows how PFM is useful in bringing out fine detail on ferroelectric polymer nanomesas.

    Time-dependent domain switching of PVDF-TrFE – (a) Topography and (b) PFM phase images of as-grown polyvinylidene fluoride-trifluoroethylene (PVDF-TrFE) nanomesa. Scan size 600 nm, Z scale 30 nm (height) and 15° (PFM phase; minimum blue, maximum yellow). (c) PFM phase image of the same nanomesa after global switching due to a DC bias of +6 V. (d-f) Time-dependent polarization orientation switching from an applied voltage pulse of -5 V after (d) 1 s, (e) 4 s, and (f) 8 s. The approximate tip position is indicated by the black dot in (a). The high electromechanical activity of PVDF-TrFe makes it attractive in many transducer and sensor applications. Imaged with the MFP-3D AFM. Adapted from Ref. 10.

    Figure 13: Time-dependent domain switching of PVDF-TrFE – (a) Topography and (b) PFM phase images of as-grown polyvinylidene fluoride-trifluoroethylene (PVDF-TrFE) nanomesa. Scan size 600 nm, Z scale 30 nm (height) and 15° (PFM phase; minimum blue, maximum yellow). (c) PFM phase image of the same nanomesa after global switching due to a DC bias of +6 V. (d-f) Time-dependent polarization orientation switching from an applied voltage pulse of -5 V after (d) 1 s, (e) 4 s, and (f) 8 s. The approximate tip position is indicated by the black dot in (a). The high electromechanical activity of PVDF-TrFe makes it attractive in many transducer and sensor applications. Imaged with the MFP-3D AFM. Adapted from Ref. 10.

    Asylum AFMs for Examining Functional Behavior
  • The ORCATM is a module in Cypher S and MFP-3D AFMs which allows current measurement at sensitive scales for CAFM. It can also make use of an optional amplifier which has low-noise and dual-gain properties, to allow measurements to be taken at high sensitivity over a range of under 1 pA to 10 µA.
  • NanoTDDBTM is another unique Asylum mode for time-dependent dielectric breakdown assessment at smaller scales than can be achieved using conventional probes. Here, the tip-sample voltage is kept constant or increased in steps to 220 V until the detection of a breakdown event.
  • Asylum has the only commercially available high-voltage PFM mode that can handle up to 220 V for use by the MFP-3D AFM and the Cypher family AFMs. All AFMs from Asylum have integrated software that offers very sensitive PFM measurements, with the Dual ACTM Resonance Tracking (DARTTM) which has been patented by Asylum, or the unique Band Excitation option.
  • Increase Output with Asylum AFMs

    This article provides a number of examples to show how powerful the use of Asylum AFMs can be in analyzing polymers, whether for scientific or engineering purposes. Newer developments have made AFMs able to acquire images to visualize a number of different physical properties and behavior as well as morphology. Asylum AFMs incorporate many remarkable functionalities, such as high spatial resolution, rapid scanning, several operating modes, and so on, which will enable many more characterizations of polymers.

    References
  • P. Samori, M. Surin, V. Palermo, R. Lazzaroni, and  P. Leclere, Phys. Chem. Chem. Phys. 8, 3927 (2006).
  • L.  Sawyer, D. Grubb, and G. Meyer, Polymer Microscopy, 3rd Edition (Springer, New York, 2008).
  • M.E.  McConney, S.  Singamaneni, and V.V.  Tsukruk,  Polym.  Rev.  50, 235 (2010).
  • H.  Schönherr and G.J.  Vancso, Scanning  Force Microscopy of Polymers  (Springer  Laboratory,  Heidelberg,  2010).
  • N.T.  Lawrence, J.M.  Kehoe, D.B.  Hoffman, C.  Marks,    J.M.  Yarbrough, G.M.  Atkinson, R.A.  Register, M.J. Fasolka, and M.L. Trawick,  Macromol.  Rapid Comm.31, 1003 (2010).
  • T.  Gkourmpis, C.  Svanberg, S.K.  Kaliappan, W. Schaffer,   M.  Obadal, G.  Kandioller, and D.  Tranchida, Eur. Polym.  J.    49, 1975 (2013).
  • S.  Kienle, T. Pirzer, S.  Krysiak, M Geisler, and T. Hugel, Faraday Discuss.160, 329  (2013).
  • C.A.  Grant, A. Alfouzan, T. Gough, P.C. Twigg and P.D. Coates, Micron 44, 174 (2013).
  • L.M.  Cox, J.P.  Killgore, Z.  Li, Z.  Zhang, D.C.  Hurley, J. Xiao, and Y. Ding, Adv.  Mater.  26, 899 (2013).
  • P.  Sharma, T.J. Reece, S.  Ducharme, and A. Gruverman, Nano  Lett.11,  1970  (2011).
  • This information has been sourced, reviewed and adapted from materials provided by Asylum Research - An Oxford Instruments Company.

    For more information on this source, please visit Asylum Research - An Oxford Instruments Company.



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